Contact an Account ManagerChromatographic resolution, characterisation and quantification of VX enantiomers in hemolysed swine blood samples
Summary
Type: GC
Application #: 213470
Catalog#: 723384.25 - GC Column, FS HYDRODEX Beta-TBDAc., 0.25mm, 25m
Detection:
Conditions: Injection: solvent vent-stop-flow mode, volume 5 µL, unpacked deactivated baffled glass liner, injection time 1 min, pre-column pressure 0 bar, temperature 50 --> 260 °C, 12 °C/s (2 min), initial time 1.1 min, vent time 1.01 min, vent flow 10 mL/min, purge flow 50 mL/min, purge time 3 min
Carrier gas: helium, 1.3 mL/min
Temperature: 50 °C for 3.5 min --> 95 °C, 0.3 °C/min (15 min) --> 115 °C, 0.2 °C/min (5 min) --> 118 °C, 0.2 °C/min --> 180 °C, 10 °C/min
Authors: Reiter, G. et al.
Source: J. Chromatogr. B 873 (2008), 86–94
Details
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